Scholarly works in Petroleum engineering
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Item Evaluating the rheological properties of a synthentic based mud formulated from Avocado Pear Oil(Society of Petroleum Engineers (SPE), 2024) Ogbemudia, O.; Ayodele, E.; Akintola, S.With the oil and gas sector increasingly focusing on deep offshore drilling in challenging conditions, there is a requirement to create drilling fluids that can perform exceptionally well in such environments. It is crucial to take into account the proper disposal of drilling fluid waste in compliance with environmental regulations. Synthetic-based muds have been suggested as a viable substitute for oil-based muds. Also, the majority of studies on synthetic-based muds have concentrated on base oils that are not indigenous to the area. This study investigates the characteristics of a synthetic-based mud derived from avocado pear oil, which is a readily available and abundant resource, and determines its appropriateness for utilisation in offshore drilling activities. Avocado pear oil was obtained, subjected to transesterification, and utilised in the creation of synthetic-based muds with oil-to-water ratios of 70:30, 75:25, and 80:20, respectively. After 24 hours, it was discovered that the electrical stability remained above 400 at temperatures of 1500 °F. The sample with an oil-water ratio of 80:20 exhibited the maximum plastic viscosity at 1500 °F after 24 hours, indicating superior rheological performance at high temperatures compared to the other samples. The sample with an oil-water ratio of 80:20 exhibited the most minimal mud filter cake in comparison to all other samples, making it the optimal choice for preventing formation damage. The pH level exceeded 8, indicating its suitability for drilling operations.Item Potentials of Musa Sapientum, Solanum Tuberosum and Elaeis Guineensis as additive to water base mud(Society for Multidisciplinary & Advanced Research Techniques (SMART), 2024) Akintola, S. A.; Okunade, D.; Adeoti, P.Oil and gas sector plays vital roles in global economy and energy, and drilling operation is undoubtedly a critical component as drilling fluid is essential during drilling operations. In order to achieve safe and successful drilling operations, optimal drilling fluid is required. Drilling fluids are complex heterogeneous fluid having diverse functionality with chemical additives to enable ultimate performance. Though, these additives expensive, but none-biodegradable. This led to search for environment-friendly additive. This study explored locally sourced degradable agricultural wastes form Banana (musa sapientum) Potato,(solanum tuberosum) and Palm head (elaeis guineensis) as alternative to conventional additives in enhancing the properties of a simple water-based mud. The agricultural wastes were characterized using the FTIR and SEM-EDS, for chemical and elemental composition, respectively. Varying concentration (1g, 2g, 3g, 4g and 5g) of these additives were used at temperature 250C, 400C, 600C, and 800C and aging time of 24hours, 48 hours and 72 hours to were determine rheological and filtration properties, using the API Recommended Practice 13B-1. Results revealed that rheological and filtration properties of water-based mud improved as the concentration of additives increases. The use of these additives is not only environmentally friendly but also economically efficient than other chemical-based additives.Item Numerical modeling and investigation of flow of incompressible non-Newtonian fluids through uniform slightly deformable channel(IEEE Xplore, 2023) Alabi, O. O.; Adeaga, O. A.; Akintola, S. A.Numerical investigations of peristaltic flow of three non-Newtonian viscous fluids arising within modelled gut were performed to show their thermal and hydrodynamic behaviour in the gut. A 3-D numerical model of the human intestine was derived using Autodesk Inventor 2017 and simulated using ANSYS FLUENT 16.0. Thyme and produced Ogi, Soymilk and Sobo are considered working fluids. The density and viscosity of the produced fluid were determined experimentally, while the density and viscosity of the digester were obtained from previous work. The results of the experiments carried out showed that the densities of the produced fluid supplements were; 1024 kg/𝑚3 , 920 kg/𝑚3and 800 kg/𝑚3 for Ogi, soybean milk and sobo respectively; their equivalent viscosities were; 1.095 Pa.s, 0.95 Pa.s, and 0.316 Pa.s. From the results, it can be seen that the velocity behaviour of the four fluids is similar, as is the thermal behaviour. The results also showed that at inlet velocity of 0.005 m/s, Ogi had the largest pressure change of 25 Pa and a heat transfer of Nu=9, while sobo had the smallest heat transfer of Nu=9 among the three fluid supplements produced. Nu=5.Item Effect of Sodium Carboxymethyl Cellulose from Delonix regia Sawdust on rheological and filtration properties of water based drilling fluid(Society of Petroleum Engineers, 2021) Imohiosen, O. U.; Akintola, S. A.Over the past years, there has been an increase in the importation of Sodium Carboxymethyl cellulose (CMC), an important drilling mud polymer additive, in the Nigerian oil and gas industry. However, the ripple effects of the importation of this polymer and other oilfield chemicals on the Nigeria oil and gas industry includes rising cost of oil and gas field development, limited oil and gas industry growth, and capital flight. In order to mitigate this trend, studies on the use of local substitutes such as starch and its derivatives have gathered momentum with risk such as competition with food supply and increase in food cost. The use of sawdust wastes which offers a non-competing and a cheap source of feedstock in the production of CMC have rarely been investigated. The study therefore investigated production of CMC from sawdust waste of a highly underutilized wood (Delonix regia), after which drilling mud tests were conducted to determine the rheological and filtration properties of mud treated with the CMC products. The CMC production adopted the Williamson ether synthesis process in a slurry medium involving two main reactions of mercerization and etherification. All reaction parameters were held constant except the etherifying agent concentration. The CMC products were characterized using FTIR Spectroscopy. The synthesized carboxymethyl cellulose products yielded good filtration and rheological properties suitable for drilling fluid applications. The use of low concentrations of about 0.5g to 1.0g of the synthesized products per laboratory barrel of mud could reduce filtration volume by 11.4% to 32.9% at low temperature and pressure conditions. The synthesized CMC products obtained from this work can be used as local substitute of low viscosity foreign CMC products.Item Development of modified fractional fluid flow equation for non–darcy flow in computer simulation of oil reservoirs(Innovative Societies & Technology Academic Multidisciplinary Society, 2021) Akintola, S. A.; Adeaga, O. A.; Muritala, O. K.Upon the depletion of oil reservoir, huge amount of oil is usually left behind. This oil, in some cases double the initial oil recovered, in order to recover the unrecovered oil, different types of secondary oil recovery techniques can be explored. A more common technique is water flooding which involve the injection of water into reservoir to displace oil into the wellbore. To determine the relative flow rates of oil and water at any point in a porous flow system while also examining factors such as fluid properties, rock properties, reservoir structural properties, pressure gradient, and flow rate which affect the displacement efficiency of a water flooding project, the fractional flow equation is employed. But the convectional fractional flow equation is applicable just to Darcy flow. The use of Darcy flow equation is not applicable in low permeability sandstone reservoir, hence non Darcy flow have been used one of such equation is the Forcheimer equation, as a result this study is aimed at modifying the Forcheimer equation and validating the new fractional flow equation using literature . The result obtained showed that the proposed equation predicts better than Forcheimer equationItem TECHNICAL AND ECONOMIC EVALUATION OF NANOFLUID ALTERNATING-BRINE FLOODING FOR ENHANCED OIL RECOVERY IN NIGER DELTA RESERVOIRS(2022-02) OMOTOSHO, Y.ANanofluid flooding in the petroleum industry has generated growing interest because of its potential to greatly improve oil recovery. However, studies have reported that injection of nanofluid could lead to impaired permeability due to adsorption of nanoparticles on reservoir rocks thereby incurring high costs. The use of single Nanofluid Flooding (NF) has not appreciably reduced permeability impairment. This study was therefore, designed to investigate the technical and economic viability of Nanofluid-Alternating-Brine Flooding (NABF) for enhanced oil recovery in Niger Delta reservoirs. Eight sandstone core samples obtained from Niger Delta, were characterised for porosity and permeability using Helium-Porosimeter and Permeameter, respectively. Densities and viscosities of crude oil samples and brine (Salinity: 32.2g/L) were determined using pycnometer and viscometer, respectively. Core samples were initially saturated with brine and drained with crude oil, to determine the initial Water Saturation (SWi). Silica nanoparticles of size: 20-70 nm, were dispersed in brine at concentrations ranging from 0.01 to 3.00 wt%. Interfacial Tensions (IFT) between oil and nanofluids were measured. Brine Flooding (BF) of core samples was conducted at 2.00 cm3 /min. The Optimum Concentration (OC) and Optimum Injection Rate (OIR) during NF were determined by injecting each nanofluid concentration at 0.50, 1.00, 2.00 and 3.00 cm3 /min. The NABF was carried out at OC and OIR. The Oil Recovery Factors (ORF) for all experiments were computed using material balance. The images of pre-flooded and post-flooded core samples were obtained using Scanning Electron Microscope. Nanoskin factors (Sn) were determined for NF and NABF and compared with the analytical model developed from Darcy’s equation. The ORFobtained were upscaled for field application and evaluated for Threshold Oil Price (TOP). Risk analysis with varying ORF, Capital Expenditure (CAPEX) and Operating Expenses (OPEX) was carried out using a commercial software. Data were analysed using ANOVA at 𝛼0.05. Porosity and liquid permeability for the samples were 17.0-30.0% and 1.1x10-8 -1.6x10-8 cm2 (1104.9-1584.0 md), respectively. The densities of crude oil and brine were 0.88 and 1.02 g/cm3 , while their viscosities were 3.0x10-4 kgms-2 (3.0 cp) and 1.0x10-4 kgms-2 (1.0 viii cp), respectively. The SWi were 11.0-18.4%. The IFT were 1.9x10-2 -2.3x10-2 N/m (18.5- 23.0 dynes/cm) while the OC and OIR for NF were 2.00 wt % and 2.00 cm3 /min, respectively. The ORF for BF, NF and NABF were 68.9-73.1, 63.8-66.2 and 83.8-86.2%, respectively. The pre-flooded cores had evenly distributed grain matrices void of external particles while permeability impairment was observed for NF. Permeability impairment reversal was observed during NABF. The predictive model for Sn agreed with the experimental result. Economic analysis revealed that for unit CAPEX (N13,985.56/bbl; $34.00/bbl) and OPEX (N1,867.48/bbl; $4.54/bbl), at discount rate of 10.0%, TOP was N20,196.79/bbl ($49.10/bbl). Risk analysis on profitability showed that TOP for proved, probable and possible ORF were 33,400.81, 19,197.24 and N12,545.87/bbl (81.20, 46.67 and $30.50/bbl), respectively. The order of impact of the economic variables on profitability was ORF>CAPEX>OPEX. Improved oil recovery in Niger Delta reservoirs was achieved using nano-alternating-brine flooding with minimal permeability impairment. The method is also profitable within the stipulated oil price regime.Item DEVELOPMENT OF A REAL-TIME PETROLEUM PRODUCTS ADULTERATION DETECTOR FOR LIQUID AND PARTICULATE CONTAMINANTS(2022-12) OLOTU, O.OAdulteration of petroleum products with the resultant safety, health, environmental and economic impact on the end-users is a challenge in Nigeria and many developing countries. The current commonly used techniques by regulatory agencies and some end-users for quality assurance of the petroleum products are time-consuming and expensive. The development and use of real-time adulterated petroleum products detector in Nigeria will therefore alleviate these problems. This study was therefore designed to develop a device for real-time detection of petroleum products adulterated with liquid and particulate contaminants. Pure samples of Premium Motor Spirit (PMS), Automotive Gas oil (AGO) and Dual Purpose Kerosene (DPK) were collected from some major petroleum products marketers. Samples of distilled water, naphtha, commercial ethanol, pure and used commercial lubricating oil, and High Pour Fuel Oil (HPFO) were also obtained and used as liquid contaminants; while sawdust, ash and fine-grain sand were used as solid particulates. At temperatures 23:1:28oC, binary mixtures of the products mixed with liquid contaminants were prepared (100:0, 95:5, 85:15, 75:25, 70:30, 65:35 … 15:85, 5:95,0:100 v/v). Likewise, a fixed volume of pure petroleum products was mixed with varying quantity of solid particulates (0, 2, 4, 6, 8, 10 g). The specific Gravity (SG) and Interfacial Tension (IFT) of the pure samples, binary mixtures were determined according to ASTM D1298 and D971 standards, respectively. These physiochemical properties (SG and IFT) of pure and contaminated fuel samples were used to develop a mathematical model. The model was then simulated into a microcontroller-based detector. A microcontroller of PIC16f876 microchip with multiple input/output pins and a load cell sensor with real-time response was used. The microcontroller takes the reading of the weight of liquid from the sensor to get the SG and IFT of the liquid in real-time. Values of SG and IFT of pure and contaminated samples of petroleum products were obtained using the developed adulteration detector and compared with laboratory measurements and those obtained using Kay’s mixing rule. Data were analysed using ANOVA at α 0.05. The SG and IFT (dynes/cm) of the pure samples were (PMS) 0.833, 47.0; (AGO) 0.812, 28.0; (DPK) 0.803, 25.0, for liquid contaminants ranged from (PMS) 0.853-0.890, 44.6-25.0; (AGO) 0.807-0.804, 46.2-29.5; (DPK) 0.811-0.947, 46.4-38.0 and for solid contaminants ranged from (PMS) 0.887-0.910, 47.8-27.2; (AGO) 0.884-0.887, 29.2-30.0; (DPK) 0.817-0.857, 25.8-32.8, respectively. The SG and IFT from Kay’s mixing rule ranged from (PMS) 0.851-0.900, 48.4-25.6; (AGO) 0.850-0.871, 40.1-35.4; (DPK) 0.864-0.881, 42.4-36.4, respectively. Adulteration of products was detected at 20.0-30.0% by volume and 10.0-20.0% by mass of contamination, respectively. The designed adulteration detector responded to the sample in real-time of 3-5s, displayed GREEN and RED for pure and adulterated samples, respectively, with their numerical SG values within ±0.01% of actual measurements. There was no significant difference between the actual and detected SG and IFT of the adulterated samples. A device that detects petroleum products adulteration in real-time and ambient temperature was developed. The method can be adapted to real-time evaluation of similar binary mixtures.Item Improving the rheological and filtration properties of an invert emulsion mud using a locally sourced modified polymer(2022) Akintola, S.A.; Sanusi, H.; Oyelola, C.Drilling fluid is designed for easy to use, cost effective and environmentally friendly. Several studies have been carried out on the use of local materials such as starch as suitable substitute for imported additives. Due to this short coming resulting from the use of native starch, the potatoes starch was chemically modified using the process of graft copolymerization, before being investigated as an additive for treatment of invert emulsion drilling. Three mud samples labelled (Base fluid, Copolymer 1 and Copolymer 2) were prepared and diesel labelled Base fluid served as control. Varying concentration of additives (1.0 and 2.0 g) were used at added to the different mud samples and laboratory study was carried out using the API Recommended Practice at varying temperature. This study is aimed at improving the properties of an invert emulsion mud using chemically modified locally sourced pomoea batatas as additiveItem Corrosion protection by novel conversion coatings on structural AI 6061(2022) Oki, M.; Adediran, A. A.; Ikechukwu, A.; Onokohwomo, C. O.; Bosa, C.; Akintola, S. A.; Adesina, O. S.Chromate conversion coatings have witnessed limited acceptability in recent times. The coatings contain Cr (VI) species that have been classified as environmental hazards and injurious to human. Thus, the use of environment-friendly and non-carcinigenic novel inorganic- inorganic hybrid conversion coatings are being explored. Vanadate (VCC), hybrid Vanadate/Molydate (HCC) conversion coatings on A16061 have been classified in terms of corrosion and adhesion performance with reference to the untreated alloy. Natural exposure tests in the atmosphere and stanant near-neutral 3.5% sodium chloride solution, as well as patentio-dynamic polarization measurements showed that the corrosion rate for HCC is lower for Vanadate, which in turn outclassed the ‘bare’ alloy. However, clusters of passive incipient pits were revealed on the former after 120 h of exposure in stagnant chloride solution. Both conversion coatings outperformed the untreated aluminiun alloy after atmospheric corrosion and adhesion tests.Item Investigation of the effect of some salts on the rheological properties of xanthan gum and gum arabic present in a drilling fluid(2022) Okaome, P.; Akintola, S.The rheological properties of a drilling fluid are important because they allow for extensive examination of the viscosity, fluid flow profile, pressure loss, equivalent circulation density, and hole cleaning capability making it the foundation for all wellbore hydraulics. The viscosity, gel strength, and yield point of Gum Arabic and Xanthan Gum contained in a fresh water-based drilling fluid were investigated in the presence of three distinct salts: calcium chloride (CaCl2), potassium chloride (KCl), and sodium chloride (NaCl). The salts were introduced separately to three distinct fresh water-based drilling fluid samples in increasing weights. The Fann V-G viscometer was used for the required rheology properties measuring the RPM and gel strength. The plastic viscosity, apparent viscosity, and yield point were calculated from the experimental data. With increasing the salt concentration, the plastic viscosity, apparent viscosity, yield point, and gel strength all decreased, which was observed for all three salts used. This research aimed to investigate the effect of three different salts; Calcium chloride (CaCl2), Potassium Chloride (KCl), and Sodium Chloride (NaCl) on the rheological properties of Gum Arabic and Xanthan Gum viscosified water-based drilling fluid.